Single Crystal XRD

Bruker Smart Apex II Ultra

Description: Minimum booking hours: 12 hours, Sample characterizing temperature Range: 80 K – 500 K, Measurement: Crystal structure determination and electron density mapping.

The instrument is used to measure single crystal XRD at various temperature (80K – 500K) using liquid nitrogen. Due to its high operating power even very small crystals can be measured (crystal size 0.1 to 0.5 mm).

Specifications

Rotating anode, Molybdenum source
Collimator diameter 0.5 mm
Maximum operating power: 45 kV 80 mA
Oxford liquid nitrogen cryostat with temperature controller
Detector: CCD detector (Apex II) with a fixed distance of 58.2 mm
3-axis goniometer with fixed Kappa axis

Room temperature

Variable temperature

Bruker Kappa Apex II

Description: Minimum booking hours: 12 hours, Single Crystal X-ray Diffractometer, Sample characterizing temperature Range: 80 K – 400 K, Measurement: Crystal structure determination.

The instrument is used to measure single crystal XRD data at various temperature (80 K – 400 K) using liquid nitrogen. Detector distance can be changed depending on the requirement (crystal size 0.3 to 0.5 mm).

Specifications

Sealed tube anode, Molybdenum source
Maximum operating power: 40 kV 30 mA
Collimator diameter 0.35 mm
Oxford liquid nitrogen cryostat with temperature controller
Detector: CCD detector (Apex II)
4-axis goniometer

Room temperature

Variable temperature

Bruker D8 Quest

Description: Minimum booking hours: 12 hours, Single Crystal X-ray Diffractometer, Sample characterizing temperature Range: 80 K – 400 K, Measurement: Crystal structure determination, Phase transition, and electron density mapping.

Specifications

Sealed tube, Molybdenum source
Collimator diameter 0.6 mm
Maximum operating power: 45 kV 30 mA
Oxford liquid nitrogen cryostat with temperature controller
Detector: Photon II detector
3-axis goniometer with fixed Kappa axis

Room temperature

Variable Temperature